Detail publikace

Application of imaging spectroscopic reflectometry for characterization of gold reduction from organometallic compound by means of plasma jet technology

VODÁK, J. NEČAS, D. PAVLIŇÁK, D. MACÁK, J. ŘIČICA, T. JAMBOR, R. OHLÍDAL, M.

Anglický název

Application of imaging spectroscopic reflectometry for characterization of gold reduction from organometallic compound by means of plasma jet technology

Typ

článek v časopise ve Web of Science, Jimp

Jazyk

en

Originální abstrakt

This work presents a new application of imaging spectroscopic reflectometry to determine a distribution of metallic gold in a layer of an organogold precursor which was treated by a plasma jet. Gold layers were prepared by spin coating from a solution of the precursor containing a small amount of polyvinylpyrrolidone on a microscopy glass, then they were vacuum dried. A difference between reflectivity of metallic gold and the precursor was utilized by imaging spectroscopic reflectometry to create a map of metallic gold distribution using a newly developed model of the studied sample. The basic principle of the imaging spectroscopic reflectometry is also shown together with the data acquisition principles. XPS measurements and microscopy observations were made to complete the imaging spectroscopic reflectometry results. It is proved that the imaging spectroscopic reflectometry represents a new method for quantitative evaluation of local reduction of metallic components from metaloorganic compounds.

Anglický abstrakt

This work presents a new application of imaging spectroscopic reflectometry to determine a distribution of metallic gold in a layer of an organogold precursor which was treated by a plasma jet. Gold layers were prepared by spin coating from a solution of the precursor containing a small amount of polyvinylpyrrolidone on a microscopy glass, then they were vacuum dried. A difference between reflectivity of metallic gold and the precursor was utilized by imaging spectroscopic reflectometry to create a map of metallic gold distribution using a newly developed model of the studied sample. The basic principle of the imaging spectroscopic reflectometry is also shown together with the data acquisition principles. XPS measurements and microscopy observations were made to complete the imaging spectroscopic reflectometry results. It is proved that the imaging spectroscopic reflectometry represents a new method for quantitative evaluation of local reduction of metallic components from metaloorganic compounds.

Klíčová slova anglicky

Gold reduction; Imaging spectroscopic reflectometry; Organometallic compound; Plasma jet

Vydáno

28.02.2017

Nakladatel

Elsevier B.V.

ISSN

0169-4332

Číslo

396

Strany od–do

284–290

Počet stran

6

BIBTEX


@article{BUT129821,
  author="Jiří {Vodák} and David {Nečas} and David {Pavliňák} and Jan M. {Macák} and Tomáš {Řičica} and Roman {Jambor} and Miloslav {Ohlídal},
  title="Application of imaging spectroscopic reflectometry for characterization of gold reduction from organometallic compound by means of plasma jet technology",
  year="2017",
  number="396",
  month="February",
  pages="284--290",
  publisher="Elsevier B.V.",
  issn="0169-4332"
}